The aim of the present work is to synthesis new magnetocaloric, magnetoelectric, piezoelectric and photochromic smart materials with improving the preparation conditions. It is well known; that Smart materials are designed materials that have a change in one or more properties in response to external stimuli. A second generation of specially machine with articulated robotic arm designed to prepare the samples with accurate physical parameters such as heating/cooling temperature, pressure, pH value and time of process. In addition, the system used to characterize the samples by measuring some of the thermal, magnetic, electrical, optical and mechanical properties.